R. J. QUINN,[A] Midland Chemical Co., Argo, Ill.
PAUL RUDNICK, Armour and Co., Chicago, Ill.
L. M. TOLMAN, Wilson and Co., Chicago, Ill.
E. TWITCHELL,[A] Emery Candle Co., Cincinnati, Ohio.
J. J. VOLLERTSEN, Morris and Co., Chicago, Ill.
Scope, Applicability and Limitations of the Methods.
These methods are intended to aid in determining the commercial valuation of fats and fatty oils in their purchase and sale, based on the fundamental assumption commonly recognized in the trade, namely, that the product is true to name and is not adulterated. For methods for determining the identity of oils and fats, the absence of adulterants therein and for specific tests used in particular industries, the chemist is referred to standard works on the analysis of fats and oils.
The methods are applicable in commercial transactions involving fats and fatty oils used in the soap, candle and tanning industries, to edible fats and oils and to fats and fatty oils intended for lubricating and burning purposes. The methods are applicable to the raw oils used in the varnish and paint industry with the exceptions noted under limitations, but special methods have not been included.
The methods have not been developed with special reference to waxes (beeswax, carnauba wax, wool wax, etc.) although some of them may be found applicable to these substances. The Committee considers the Wijs method superior to the Hanus method for the determination of iodine number of linseed oil as well as other oils, although the Hanus method has been considered standard for this work for some time and has been adopted by the American Society for Testing Materials and in various specifications. It has been customary to use the Hübl method for the determination of iodine value of tung oil (China wood oil) but the Committee's work indicates that the Wijs method is satisfactory for this determination.
1. SAMPLING WHILE LOADING--Sample shall be taken at discharge of pipe where it enters tank car dome. The total sample taken shall be not less than 50 lbs. and shall be a composite of small samples of about 1 pound each, taken at regular intervals during the entire period of loading.
The sample thus obtained is thoroughly mixed and uniform 3-lb. portions placed in air-tight 3-lb. metal containers. At least three such samples shall be put up, one for the buyer, one for the seller, and the third to be sent to a referee chemist in case of dispute. All samples are to be promptly and correctly labeled and sealed.